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Methods, Problems and Solutions

Possible binders for powder diffraction samples and affixing powders to zero background plates

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Query on binders to afix powder samples to low background plates/zero background plates (and stubs) which do not give appreciable contribution to the diffraction pattern

Additions, comments, suggestions are appreciated

From: "Madsen, Ian (Minerals, Clayton)" [[email protected]]
To: "'L. Cranswick'" [[email protected]]
Subject: RE: Query on Acetyl Acetate
Date: Fri, 15 Dec 2000 09:59:15 +1100

Hi Again,

An XRF person has just entered my office. The current favourite is Elvacite
(an acrylic resin - mix 10% in turpentine). Another option is PolyVinyl
Alcohol (PVA - mix powder in a water/ethanol) 

Cheers again

-----

Hi,

I don't recall ever using anything except ethanol or acetone to make a
slurry for use on ZBP's. However, I think the material you might be thinking
of is Methyl Methacrylate - the XRF guys use it as a pressed powder sample
binder. I will ask them later to discover their current favourite.

Cheers

o----------------------oo0oo---------------------------o
     Ian Madsen
        CSIRO Minerals
        Box 312
        Clayton South    3169
        Victoria
        AUSTRALIA

     Phone	+61 3 9545 8785  direct
		+61 3 9545 8500  switch
		0417 554 935   mobile
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     Email  [email protected]
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